3Q03
Crystal structure of plasminogen activator inhibitor-1 in a metastable active conformation.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2009-10-12 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.28 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 76.680, 67.160, 91.160 |
Unit cell angles | 90.00, 100.45, 90.00 |
Refinement procedure
Resolution | 19.758 - 2.640 |
R-factor | 0.1742 |
Rwork | 0.172 |
R-free | 0.22540 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1dvm |
RMSD bond length | 0.003 |
RMSD bond angle | 0.699 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.6_289)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.750 |
High resolution limit [Å] | 2.600 | 2.640 |
Number of reflections | 54546 | |
<I/σ(I)> | 2.03 | |
Completeness [%] | 99.1 | 99.6 |
Redundancy | 3.2 | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.1 | 293 | 1.7 - 3.0 M NaCl, 5 mM Mes pH 6.1, VAPOR DIFFUSION, HANGING DROP, temperature 293K |