Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-05-15 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 1.0000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 70.530, 61.890, 70.140 |
Unit cell angles | 90.00, 112.54, 90.00 |
Refinement procedure
Resolution | 42.520 - 1.340 |
R-factor | 0.1274 |
Rwork | 0.127 |
R-free | 0.14271 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.332 |
Refinement software | REFMAC (5.6.0041) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.520 | 1.360 |
High resolution limit [Å] | 1.340 | 1.340 |
Number of reflections | 119377 | |
<I/σ(I)> | 11.9 | 2.4 |
Completeness [%] | 99.7 | 90.3 |
Redundancy | 3.6 | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 300 | 0.1M Tris-HCl pH 8.0, 1.8M (NH4)2SO4, VAPOR DIFFUSION, SITTING DROP, temperature 300.0 K |