3B9K
Crystal structure of CD8alpha-beta in complex with YTS 156.7 FAB
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL11-1 |
Synchrotron site | SSRL |
Beamline | BL11-1 |
Temperature [K] | 93.2 |
Detector technology | CCD |
Collection date | 2005-07-16 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97945 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 91.779, 92.747, 190.310 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.330 - 2.700 |
R-factor | 0.238 |
Rwork | 0.235 |
R-free | 0.28400 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.015 |
RMSD bond angle | 1.576 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.800 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.131 | 0.579 |
Number of reflections | 45395 | |
<I/σ(I)> | 9.6 | 2.17 |
Completeness [%] | 97.5 | 99.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | sitting drop | 6.2 | 296 | PEG 8000, 0.1 M Na/K phosphate, 0.2 M NaCl, pH 6.2, sitting drop, temperature 296K |