2YQ7
Structure of Bcl-xL bound to BimLOCK
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-08-08 |
Detector | ADSC QUANTUM 315r |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 73.803, 35.223, 61.363 |
Unit cell angles | 90.00, 101.12, 90.00 |
Refinement procedure
Resolution | 34.068 - 1.901 |
R-factor | 0.1653 |
Rwork | 0.163 |
R-free | 0.20780 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3FDL CHAIN A |
RMSD bond length | 0.006 |
RMSD bond angle | 0.941 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.090 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.100 | 0.550 |
Number of reflections | 12014 | |
<I/σ(I)> | 20.3 | 2 |
Completeness [%] | 96.8 | 80.1 |
Redundancy | 6.1 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 15 % (W/V) PEG 400, 5 % PEG 3000, 10 % GLYCEROL AND 0.1 M MES PH 6.5. |