2RJE
Crystal structure of L3MBTL1 in complex with H4K20Me2 (residues 17-25), orthorhombic form II
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ DW |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2006-12-18 |
Detector | RIGAKU RAXIS |
Wavelength(s) | 1.54000 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 109.894, 124.640, 90.031 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.480 - 1.860 |
R-factor | 0.19292 |
Rwork | 0.191 |
R-free | 0.23131 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2pqw |
RMSD bond length | 0.016 |
RMSD bond angle | 1.444 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 37.480 |
High resolution limit [Å] | 1.860 |
Rmerge | 0.085 |
Number of reflections | 103400 |
Redundancy | 6.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.4 | 300 | 6% PEG 3350, 0.1M Ammonium sulfate, 20% Glycerol, 0.1 M Sodium acetate pH 4.4 , VAPOR DIFFUSION, HANGING DROP, temperature 300K |