2RFN
x-ray structure of c-Met with inhibitor.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ SUPERBRIGHT |
Temperature [K] | 130 |
Detector technology | IMAGE PLATE |
Collection date | 2004-08-20 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 74.509, 78.919, 129.128 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.500 |
R-factor | 0.24061 |
Rwork | 0.238 |
R-free | 0.29414 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1r1w |
RMSD bond length | 0.009 |
RMSD bond angle | 1.254 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.590 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.073 | 0.403 |
Number of reflections | 24997 | |
<I/σ(I)> | 20.5 | 2.8 |
Completeness [%] | 97.5 | 95.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 5 | 298 | 12% PEG 6000, 1.0M LiCl2, 0.1M sodium citrate, pH 5.0, VAPOR DIFFUSION, temperature 298K |