2PIV
Androgen receptor with small molecule
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-07-16 |
Detector | ADSC QUANTUM 210 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 56.400, 66.020, 72.700 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.000 - 1.950 |
Rwork | 0.230 |
R-free | 0.25000 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | ELVES |
Data scaling software | ELVES |
Phasing software | CNS |
Refinement software | ELVES |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | |
High resolution limit [Å] | 1.950 | 1.950 |
Rmerge | 0.065 | 0.065 |
Number of reflections | 20097 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | VAPOR DIFFUSION, SITTING DROP, temperature 298K |