2IWZ
Human mitochondrial beta-ketoacyl ACP synthase complexed with hexanoic acid
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X11 |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | X11 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-10-31 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 71.912, 95.920, 114.637 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.310 - 1.650 |
R-factor | 0.156 |
Rwork | 0.155 |
R-free | 0.18800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1w0i |
RMSD bond length | 0.010 |
RMSD bond angle | 1.277 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.300 | 1.550 |
High resolution limit [Å] | 1.500 | 1.480 |
Rmerge | 0.090 | 0.740 |
Number of reflections | 132820 | |
<I/σ(I)> | 5.4 | 1 |
Completeness [%] | 97.0 | 79.7 |
Redundancy | 5.4 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.8 | 24% PEG3350, 0.2M NH4CL, pH 7.80 |