1C2O
ELECTROPHORUS ELECTRICUS ACETYLCHOLINESTERASE
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 293 |
| Detector technology | IMAGE PLATE |
| Collection date | 1996-06-15 |
| Detector | MARRESEARCH |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 211.160, 129.750, 195.420 |
| Unit cell angles | 90.00, 103.20, 90.00 |
Refinement procedure
| Resolution | 12.000 - 4.200 |
| Rwork | 0.375 |
| R-free | 0.38500 |
| Data reduction software | DENZO |
| Data scaling software | SCALA |
| Phasing software | AMoRE |
| Refinement software | CNS |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 12.000 |
| High resolution limit [Å] | 4.200 |
| Rmerge | 0.180 |
| Total number of observations | 158367 * |
| Number of reflections | 24590 |
| Completeness [%] | 66.0 |
| Redundancy | 1.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 5.5 | 20 * | 1.4 M ammonium sulfate, VAPOR DIFFUSION, temperature 298K, pH 5.5 |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | reservoir | ammonium sulfate | 1.4 (M) |
