6QXV
Pink beam serial crystallography: Proteinase K, 1 us exposure, 1585 patterns merged (2 chips)
Summary for 6QXV
| Entry DOI | 10.2210/pdb6qxv/pdb |
| Descriptor | Proteinase K, CALCIUM ION, SULFATE ION, ... (5 entities in total) |
| Functional Keywords | pink beam, fixed-target, serial crystallography, proteinase k, hydrolase |
| Biological source | Parengyodontium album (Tritirachium album) |
| Total number of polymer chains | 1 |
| Total formula weight | 30202.00 |
| Authors | Tolstikova, A.,Oberthuer, D.,Meents, A. (deposition date: 2019-03-08, release date: 2019-09-25, Last modification date: 2024-11-06) |
| Primary citation | Tolstikova, A.,Levantino, M.,Yefanov, O.,Hennicke, V.,Fischer, P.,Meyer, J.,Mozzanica, A.,Redford, S.,Crosas, E.,Opara, N.L.,Barthelmess, M.,Lieske, J.,Oberthuer, D.,Wator, E.,Mohacsi, I.,Wulff, M.,Schmitt, B.,Chapman, H.N.,Meents, A. 1 kHz fixed-target serial crystallography using a multilayer monochromator and an integrating pixel detector. Iucrj, 6:927-937, 2019 Cited by PubMed Abstract: Reliable sample delivery and efficient use of limited beam time have remained bottlenecks for serial crystallography (SX). Using a high-intensity polychromatic X-ray beam in combination with a newly developed charge-integrating JUNGFRAU detector, we have applied the method of fixed-target SX to collect data at a rate of 1 kHz at a synchrotron-radiation facility. According to our data analysis for the given experimental conditions, only about 3 000 diffraction patterns are required for a high-quality diffraction dataset. With indexing rates of up to 25%, recording of such a dataset takes less than 30 s. PubMed: 31576225DOI: 10.1107/S205225251900914X PDB entries with the same primary citation |
| Experimental method | X-RAY DIFFRACTION (1.94 Å) |
Structure validation
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