9ZYV

[asym] Two turn tensegrity triangle exhibiting hyperasymmetry

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 17-ID
Synchrotron site	APS
Beamline	17-ID
Temperature [K]	100
Detector technology	PIXEL
Collection date	2022-07-24
Detector	DECTRIS EIGER X 9M
Wavelength(s)	1.00743
Spacegroup name	P 1
Unit cell lengths	67.329, 68.980, 68.898
Unit cell angles	81.13, 85.36, 65.16

Refinement procedure

Resolution	34.030 - 4.100
R-factor	0.261
Rwork	0.259
R-free	0.29460
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	0.752
Data reduction software	autoPROC
Data scaling software	STARANISO
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	68.064	68.064	4.586
High resolution limit [Å]	4.098	13.123	4.098
Number of reflections	5167	258	258
<I/σ(I)>	4.8
Completeness [%]	85.3
Redundancy	3.6
CC(1/2)	0.998	0.997	0.309

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	8	293	100 mM MOPS, 1.25 M magnesium sulfate