9ZXK

[a3T17] Asymmetric three turn tensegrity triangle with psuedosymmetry

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 17-ID
Synchrotron site	APS
Beamline	17-ID
Temperature [K]	100
Detector technology	PIXEL
Collection date	2022-12-11
Detector	DECTRIS EIGER X 9M
Wavelength(s)	1.007430
Spacegroup name	P 1
Unit cell lengths	89.460, 100.603, 100.888
Unit cell angles	113.13, 110.06, 102.64

Refinement procedure

Resolution	45.400 - 5.960
R-factor	0.1499
Rwork	0.149
R-free	0.18300
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.010
RMSD bond angle	1.029
Data reduction software	autoPROC
Data scaling software	STARANISO
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	84.407	84.407	6.809
High resolution limit [Å]	5.959	19.265	5.959
Number of reflections	3825	201	202
<I/σ(I)>	5.2
Completeness [%]	83.6
Redundancy	3.6		3.8
CC(1/2)	0.999	0.999	0.470

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	8	293	100 mM MOPS, 1.25 M magnesium sulfate