9ZM8

Crystal structure of 7160 in complex with minor repeat region from circumsporozoite protein

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 5.0.2
Synchrotron site	ALS
Beamline	5.0.2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-05-02
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.98
Spacegroup name	P 21 21 21
Unit cell lengths	87.003, 101.044, 104.841
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	46.530 - 2.270
R-factor	0.2541
Rwork	0.253
R-free	0.28630
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.002
RMSD bond angle	0.515
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX ((1.21.2_5419: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.310
High resolution limit [Å]	2.270	2.270
Rpim	0.068
Number of reflections	42274	2079
<I/σ(I)>	14.7
Completeness [%]	97.7
Redundancy	6.3
CC(1/2)	0.990	0.880

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7	293	0.1 M HEPES (pH 7.0), 1 M lithium chloride, and 20% (w/v) PEG 6000.