9ZL9

Crystal structure of DCAF1 in complex with SDIPTAC C7

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-002+
Temperature [K]	100
Detector technology	PIXEL
Collection date	2025-10-08
Detector	DECTRIS EIGER R 1M
Wavelength(s)	1.54184
Spacegroup name	C 1 2 1
Unit cell lengths	147.301, 85.132, 222.550
Unit cell angles	90.00, 89.98, 90.00

Refinement procedure

Resolution	30.750 - 2.600
R-factor	0.2696
Rwork	0.269
R-free	0.31710
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.003
RMSD bond angle	0.616
Data reduction software	CrysalisPro
Data scaling software	Aimless
Phasing software	PHENIX
Refinement software	PHENIX (1.21.1_5286)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.750	2.740
High resolution limit [Å]	2.600	2.600
Rmerge	0.300	2.210
Rpim	0.144	1.045
Number of reflections	84914	12453
<I/σ(I)>	4.8
Completeness [%]	99.9
Redundancy	5.3
CC(1/2)	0.972	0.514

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7.3	294.15	0.2 M sodium fluoride, 20% w/v PEG 3350, pH 7.3