9ZG4

5jc21/CG13250 bound to BRD4-BD1.

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	MAD
Source type	SYNCHROTRON
Source details	APS BEAMLINE 21-ID-D
Synchrotron site	APS
Beamline	21-ID-D
Temperature [K]	296
Detector technology	PIXEL
Collection date	2016-08-26
Detector	DECTRIS EIGER X 9M
Wavelength(s)	1.1
Spacegroup name	P 21 21 21
Unit cell lengths	41.772, 59.480, 108.162
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	40.010 - 1.480
R-factor	0.1946
Rwork	0.193
R-free	0.22790
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.128
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	54.800	1.560
High resolution limit [Å]	1.480	1.480
Number of reflections	275217	44857
<I/σ(I)>	13.6	2.5
Completeness [%]	90.6	100
Redundancy	6.6	6.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		296	100 mM Magnesium Formate and 15% PEG 3350.