9YBX

ARID1B ARID bound to compound C-1 (5-fluoro-2-(1H-pyrrolo[2,3-b]pyridine-3-sulfonamido)benzoic acid)

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	CLSI BEAMLINE 08ID-1
Synchrotron site	CLSI
Beamline	08ID-1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2023-11-16
Detector	DECTRIS EIGER X 9M
Wavelength(s)	0.916829
Spacegroup name	P 65
Unit cell lengths	68.679, 68.679, 46.085
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	36.430 - 1.450
R-factor	0.1684
Rwork	0.166
R-free	0.19050
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.018
RMSD bond angle	1.667
Data reduction software	autoPROC
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	36.430	1.500
High resolution limit [Å]	1.450	1.450
Rmerge	0.103	2.018
Rpim	0.023
Number of reflections	21863	2144
<I/σ(I)>	15.3	2.2
Completeness [%]	99.1	98.39
Redundancy	20.21	20.9
CC(1/2)	0.998	0.763

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		277	1.5 M sodium citrate, pH 6.5, 0.033% w/v 4-nitrobenzoic acid, 0.033% w/v 5-sulfosalicylic acid dihydrate, 0.033% w/v naphthalene-1,3,6-trisulfonic acid trisodium salt hydrate, 0.002 M HEPES sodium, pH 6.8