9YBT

ARID1B ARID bound to compound A-2 (5-(hex-1-yn-1-yl)-3-methylpyridin-2(1H)-one)

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	CLSI BEAMLINE 08ID-1
Synchrotron site	CLSI
Beamline	08ID-1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2023-11-10
Detector	DECTRIS EIGER X 9M
Wavelength(s)	0.95355
Spacegroup name	P 65
Unit cell lengths	69.135, 69.135, 46.041
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	36.500 - 1.440
R-factor	0.1624
Rwork	0.161
R-free	0.17990
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.013
RMSD bond angle	1.323
Data reduction software	autoPROC
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	36.500	1.490
High resolution limit [Å]	1.440	1.440
Rmerge	0.090	2.266
Rpim	0.020
Number of reflections	22747	2228
<I/σ(I)>	17.8	1.9
Completeness [%]	100.0	100
Redundancy	20.02	20.55
CC(1/2)	0.999	0.714

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	6.5	277	1.5 M sodium citrate, pH 6.5, 0.033% w/v 4-nitrobenzoic acid, 0.033% w/v 5-sulfosalicylic acid dihydrate, 0.033% w/v naphthalene-1,3,6-trisulfonic acid trisodium salt hydrate, 0.002 M HEPES sodium, pH 6.8