9YAH

Crystal structure of metallochaperone AccA from Neisseria gonorrhoeae

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	AUSTRALIAN SYNCHROTRON BEAMLINE MX1
Synchrotron site	Australian Synchrotron
Beamline	MX1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-08-23
Detector	DECTRIS EIGER2 S 9M
Wavelength(s)	1.377
Spacegroup name	P 32 2 1
Unit cell lengths	103.863, 103.863, 31.609
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	44.970 - 2.900
R-factor	0.2228
Rwork	0.217
R-free	0.27080
Structure solution method	SAD
RMSD bond length	0.003
RMSD bond angle	0.599
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHENIX
Refinement software	PHENIX (1.21.2_5419)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	44.970	44.970
High resolution limit [Å]	2.890	2.890
Number of reflections	8469	8469
<I/σ(I)>	12.19
Completeness [%]	99.3
Redundancy	10.3
CC(1/2)	0.994	0.994

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		296	0.2 M NaCl, 25% w/v PEG3350, 0.1 M Tris (pH 8.5)