9XAR
Structure of the SARS-CoV-2 Spike N-terminal domain(NTD) in complex with the C1624 Fab
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL02U1 |
| Synchrotron site | SSRF |
| Beamline | BL02U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2024-09-15 |
| Detector | DECTRIS EIGER2 S 9M |
| Wavelength(s) | 0.97925 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 75.608, 116.030, 137.003 |
| Unit cell angles | 90.00, 104.98, 90.00 |
Refinement procedure
| Resolution | 36.170 - 2.770 |
| R-factor | 0.2421 |
| Rwork | 0.240 |
| R-free | 0.28820 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.665 |
| Data reduction software | xia2 |
| Data scaling software | xia2 |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.21.1_5286) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 38.680 | 2.840 |
| High resolution limit [Å] | 2.770 | 2.770 |
| Number of reflections | 58234 | 4264 |
| <I/σ(I)> | 12.9 | |
| Completeness [%] | 100.0 | |
| Redundancy | 6.9 | |
| CC(1/2) | 0.993 | 0.641 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 289 | 0.1 M Sodium HEPES 7.0 20 % w/v PEG 8000, 4.0% v/v Formamide |
