9X56

Crystal structure of RhoGDI2 in complex with Compound 2542

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-03-24
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.9778
Spacegroup name	P 43 21 2
Unit cell lengths	55.176, 55.176, 96.006
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	27.680 - 1.700
R-factor	0.1759
Rwork	0.174
R-free	0.21560
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	0.897
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX ((1.19rc3_4028: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	40.000	1.730
High resolution limit [Å]	1.700	1.700
Rmerge	0.102	0.584
Number of reflections	17036	826
<I/σ(I)>	31.8
Completeness [%]	100.0	100
Redundancy	18.9
CC(1/2)	0.980	0.955

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	30% PEG1500