9X55

Crystal structure of RhoGDI2 in complex with Compound 3054a

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-03-16
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.9785
Spacegroup name	P 43 21 2
Unit cell lengths	53.958, 53.958, 94.868
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	38.150 - 2.370
R-factor	0.2077
Rwork	0.205
R-free	0.26030
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.003
RMSD bond angle	0.579
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX ((1.19rc3_4028: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	40.000	2.410
High resolution limit [Å]	2.370	2.370
Rmerge	0.101	0.476
Number of reflections	6119	283
<I/σ(I)>	26.3	2.9
Completeness [%]	99.7	100
Redundancy	17.6	12.5
CC(1/2)	0.998	0.990

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	30% PEG1500