9X54

Crystal structure of RhoGDI2 in complex with Compound 3054b

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-03-16
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.9785
Spacegroup name	P 43 21 2
Unit cell lengths	55.313, 55.313, 95.148
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	36.180 - 2.130
R-factor	0.1946
Rwork	0.193
R-free	0.23370
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	0.926
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX ((1.19rc3_4028: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.170
High resolution limit [Å]	2.130	2.130
Rmerge	0.090	0.732
Number of reflections	8604	411
<I/σ(I)>	39.1
Completeness [%]	97.5	96.9
Redundancy	24.2	20.4
CC(1/2)	0.996	0.948

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	30% PEG1500