9WN6
HNHNme1-AcrIIC1BoeST
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL10U2 |
| Synchrotron site | SSRF |
| Beamline | BL10U2 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2023-12-17 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.97918 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 45.473, 110.209, 46.990 |
| Unit cell angles | 90.00, 116.16, 90.00 |
Refinement procedure
| Resolution | 40.820 - 1.700 |
| R-factor | 0.1657 |
| Rwork | 0.163 |
| R-free | 0.21310 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.933 |
| Data scaling software | XDS |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((1.19_4092: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 40.820 | 1.760 |
| High resolution limit [Å] | 1.700 | 1.700 |
| Rmerge | 0.105 | |
| Number of reflections | 42043 | 3475 |
| <I/σ(I)> | 7.1 | |
| Completeness [%] | 91.5 | |
| Redundancy | 2.9 | |
| CC(1/2) | 0.986 | 0.391 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | BATCH MODE | 289.15 | 0.1M Sodium malonate pH 4.0, 12% Polyethylene glycol 3,350 |
