9WJK

Crystal structure of mouse EOGT-UDP complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2021-09-13
Detector	DECTRIS EIGER X 16M
Wavelength(s)	1.000020
Spacegroup name	P 21 2 21
Unit cell lengths	54.914, 58.635, 179.354
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	49.080 - 1.800
R-factor	0.1708
Rwork	0.169
R-free	0.20020
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.013
RMSD bond angle	1.246
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	MOLREP
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	49.080	1.864
High resolution limit [Å]	1.800	1.800
Rmerge	0.028	0.257
Number of reflections	54653	5364
<I/σ(I)>	15.38
Completeness [%]	99.9	99.67
Redundancy	2
CC(1/2)	0.999	0.869

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	8.5	293	0.1M Tris (8.5), 25% PEG3,350