9WIV
SbSOMT in complex with SAH
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL02U1 |
| Synchrotron site | SSRF |
| Beamline | BL02U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2025-05-30 |
| Detector | DECTRIS EIGER2 S 9M |
| Wavelength(s) | 0.979 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 64.870, 94.382, 64.993 |
| Unit cell angles | 90.00, 113.71, 90.00 |
Refinement procedure
| Resolution | 59.577 - 2.900 |
| Rwork | 0.216 |
| R-free | 0.25080 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.002 |
| RMSD bond angle | 0.849 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0430 (refmacat 0.4.105)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 94.380 | 3.080 |
| High resolution limit [Å] | 2.900 | 2.900 |
| Number of reflections | 15690 | 2607 |
| <I/σ(I)> | 9.7 | |
| Completeness [%] | 97.7 | |
| Redundancy | 6.9 | |
| CC(1/2) | 0.996 | 0.656 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.04 M Citric Acid/0.06 M Bis-Tris Propane pH 6.4; 20% PEG 3350; 5% Glycerol |
