9VZU

Crystal structure of EPIC1 from Phytophthora nicotianae

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 5C (4A)
Synchrotron site	PAL/PLS
Beamline	5C (4A)
Temperature [K]	125
Detector technology	PIXEL
Collection date	2023-03-04
Detector	DECTRIS EIGER X 9M
Wavelength(s)	1.000
Spacegroup name	C 1 2 1
Unit cell lengths	92.240, 110.990, 84.290
Unit cell angles	90.00, 105.75, 90.00

Refinement procedure

Resolution	29.680 - 2.390
R-factor	0.2117
Rwork	0.209
R-free	0.25310
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.010
RMSD bond angle	1.902
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHENIX
Refinement software	PHENIX ((1.20.1_4487: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	29.680	2.475
High resolution limit [Å]	2.390	2.390
Number of reflections	32353	3235
<I/σ(I)>	27.51
Completeness [%]	99.8
Redundancy	7
CC(1/2)	1.000	0.962

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293.15	27%(w/v) PEG 3350, 0.1M BIS-TRIS, pH 6.7, 0.2M Ammonium sulfate