9VZL

Crystal structure of T2R-TTL-Tz12 complex

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-06-12
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97923
Spacegroup name	P 21 21 21
Unit cell lengths	103.870, 156.030, 179.540
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	58.890 - 2.810
R-factor	0.2508
Rwork	0.249
R-free	0.29420
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	0.852
Data reduction software	xia2
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX ((1.18.2_3874: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	58.920	2.860
High resolution limit [Å]	2.810	2.810
Number of reflections	70732	3434
<I/σ(I)>	8.9
Completeness [%]	98.6
Redundancy	12.7
CC(1/2)	0.995	0.262

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	6% PEG, 5% glycerol, 0.1 M MES, 30 mM CaCl2, 30 mM MgCl2, pH 6.7