9VZ4

Crystal structure of T2R-TTL-Tz17 complex

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-06-12
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97853
Spacegroup name	P 21 21 21
Unit cell lengths	105.450, 157.740, 180.910
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	51.780 - 2.750
R-factor	0.2303
Rwork	0.229
R-free	0.26610
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.003
RMSD bond angle	0.698
Data reduction software	xia2
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX ((???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	51.780	2.820
High resolution limit [Å]	2.750	2.750
Number of reflections	79076	5776
<I/σ(I)>	13
Completeness [%]	99.9
Redundancy	13.4
CC(1/2)	0.997	0.734

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	6% PEG, 5% glycerol, 0.1 M MES, 30 mM CaCl2, 30 mM MgCl2, pH 6.7