9VZ1

Crystal structure of T2R-TTL-Tz16 complex

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-06-12
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97861
Spacegroup name	P 21 21 21
Unit cell lengths	105.410, 157.820, 180.640
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	59.630 - 2.380
R-factor	0.2535
Rwork	0.252
R-free	0.27540
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	0.649
Data reduction software	xia2
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX ((???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	59.630	2.440
High resolution limit [Å]	2.380	2.380
Number of reflections	118279	6998
<I/σ(I)>	15.6
Completeness [%]	97.8
Redundancy	12.5
CC(1/2)	0.998	0.578

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	6% PEG, 5% glycerol, 0.1 M MES, 30 mM CaCl2, 30 mM MgCl2, pH 6.7