9VYP

Crystal structure of T2R-TTL-TZ2 complex

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-06-18
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97923
Spacegroup name	P 21 21 21
Unit cell lengths	104.740, 157.260, 179.970
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	56.050 - 2.520
R-factor	0.2699
Rwork	0.268
R-free	0.29960
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	0.727
Data reduction software	XDS
Data scaling software	xia2
Phasing software	PHASER
Refinement software	PHENIX ((???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	62.880	2.560
High resolution limit [Å]	2.520	2.520
Number of reflections	100858	5017
<I/σ(I)>	7.4
Completeness [%]	100.0
Redundancy	12.8
CC(1/2)	0.993	0.345

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	6% PEG, 5% glycerol, 0.1 M MES, 30 mM CaCl2, 30 mM MgCl2, pH 6.7