9VYK

Crystal structure of T2R-TTL-312 complex

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-06-18
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97923
Spacegroup name	P 21 21 21
Unit cell lengths	104.580, 156.930, 180.630
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	59.230 - 2.650
R-factor	0.239
Rwork	0.237
R-free	0.27110
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	0.722
Data reduction software	XDS
Data scaling software	xia2
Phasing software	PHASER
Refinement software	PHENIX ((???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	60.210	2.700
High resolution limit [Å]	2.650	2.650
Number of reflections	85766	4250
<I/σ(I)>	9.1
Completeness [%]	98.7
Redundancy	12.8
CC(1/2)	0.994	0.276

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	6% PEG, 5% glycerol, 0.1 M MES, 30 mM CaCl2, 30 mM MgCl2, pH 6.7