9UYS

Tyrosine-protein phosphatase non-receptor type 2

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-05-13
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.987
Spacegroup name	P 1 21 1
Unit cell lengths	58.290, 76.980, 78.330
Unit cell angles	90.00, 111.28, 90.00

Refinement procedure

Resolution	44.380 - 2.040
R-factor	0.1917
Rwork	0.190
R-free	0.22530
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.002
RMSD bond angle	0.549
Data reduction software	XDS
Phasing software	PHENIX
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	44.380	2.090
High resolution limit [Å]	2.040	2.040
Rmeas	0.111
Rpim	0.044
Number of reflections	39584	2413
<I/σ(I)>	11.73
Completeness [%]	96.0
Redundancy	6.1
CC(1/2)	0.997	0.648

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	6.5	289.15	4%w/v PEG 8000, 0.1 M sodium cacodylate, 40% v/v MPD