9UVR
Crystal structure of SSA1632 from Streptococcus sanguinis
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL41XU |
| Synchrotron site | SPring-8 |
| Beamline | BL41XU |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-10-23 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.900 |
| Spacegroup name | P 1 |
| Unit cell lengths | 42.033, 64.116, 92.978 |
| Unit cell angles | 78.46, 80.46, 75.77 |
Refinement procedure
| Resolution | 47.200 - 3.200 |
| R-factor | 0.2784 |
| Rwork | 0.278 |
| R-free | 0.28890 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.595 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | MOLREP |
| Refinement software | PHENIX ((1.20.1_4487: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.200 | 3.420 |
| High resolution limit [Å] | 3.200 | 3.200 |
| Number of reflections | 14942 | 9479 |
| <I/σ(I)> | 5.9 | |
| Completeness [%] | 98.8 | |
| Redundancy | 3.6 | |
| CC(1/2) | 0.982 | 0.923 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | cadmium sulfate sodium acetate trihydrate HEPES |
