9UL1
Crystal structure of Tibetan wild boar SLA-1*Z0301 for 2.32 angstrom
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL18U1 |
| Synchrotron site | SSRF |
| Beamline | BL18U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-06-18 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.97853 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 156.806, 48.428, 53.419 |
| Unit cell angles | 90.00, 100.47, 90.00 |
Refinement procedure
| Resolution | 46.246 - 2.323 |
| Rwork | 0.278 |
| R-free | 0.29400 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Data reduction software | HKL-3000 |
| Data scaling software | HKL-3000 |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0430) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 46.246 | 2.380 |
| High resolution limit [Å] | 2.320 | 2.320 |
| Rpim | 0.041 | 0.537 |
| Number of reflections | 15993 | 2373 |
| <I/σ(I)> | 15.5 | |
| Completeness [%] | 92.7 | |
| Redundancy | 3.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 291 | 25% [wt/vol] polyethylene glycol 3350, 0.2 M magnesium chloride hexahydrate, 0.1 M HEPES pH 7.5 |
