9UAW

LL-DA-4-cdk2 protein

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-03-17
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.987
Spacegroup name	P 21 21 21
Unit cell lengths	53.800, 72.000, 72.210
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	43.140 - 1.720
R-factor	0.2001
Rwork	0.197
R-free	0.24890
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	0.938
Refinement software	PHENIX ((1.20.1_4487: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	53.800	1.760
High resolution limit [Å]	1.720	1.720
Rmerge	0.145	1.448
Number of reflections	30521	2221
<I/σ(I)>	13.1
Completeness [%]	100.0
Redundancy	12.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7.4	300	20% PEG 3350, 100 mM Hepes