9UAU

CDK2_LL-DA-3

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-03-17
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.987
Spacegroup name	P 21 21 21
Unit cell lengths	53.620, 71.400, 71.840
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	50.640 - 1.470
R-factor	0.1877
Rwork	0.186
R-free	0.21880
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond angle	13.318
Refinement software	PHENIX ((1.20.1_4487: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.640	1.550
High resolution limit [Å]	1.470	1.510
Rmerge	0.059	0.464
Number of reflections	429031	9752
<I/σ(I)>	20.2
Completeness [%]	96.9
Redundancy	10

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		300	20% PEG3350,100 mM Hepes(pH = 7.4)