Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2024-04-19 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1.00000 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 73.600, 91.080, 83.170 |
| Unit cell angles | 90.00, 97.28, 90.00 |
Refinement procedure
| Resolution | 35.070 - 1.920 |
| R-factor | 0.1841 |
| Rwork | 0.183 |
| R-free | 0.22350 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.673 |
| Data reduction software | HKL-3000 |
| Data scaling software | HKL-3000 |
| Phasing software | HKL-3000 |
| Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 35.070 | 1.990 |
| High resolution limit [Å] | 1.920 | 1.920 |
| Number of reflections | 82489 | 8185 |
| <I/σ(I)> | 17.1 | |
| Completeness [%] | 90.6 | |
| Redundancy | 6.6 | |
| CC(1/2) | 0.999 | 0.784 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG 3000, ammonium sulfate, bis-tris methane |
