9T05
X-ray structure of the adduct formed by dirhodium tetraacetate with a C-phycocyanin
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2020-01-24 |
| Detector | DECTRIS PILATUS 6M-F |
| Wavelength(s) | 0.9537 |
| Spacegroup name | P 2 21 21 |
| Unit cell lengths | 60.586, 188.500, 207.212 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 139.827 - 2.169 |
| Rwork | 0.227 |
| R-free | 0.26330 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.729 |
| Data reduction software | autoPROC |
| Data scaling software | autoPROC |
| Phasing software | REFMAC |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 188.500 | 2.310 |
| High resolution limit [Å] | 2.169 | 2.170 |
| Rmerge | 0.340 | 2.130 |
| Rpim | 0.100 | 0.656 |
| Number of reflections | 102759 | 5138 |
| <I/σ(I)> | 6.6 | |
| Completeness [%] | 94.2 | 63.6 |
| Redundancy | 12.9 | 11.6 |
| CC(1/2) | 0.996 | 0.564 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | 0.1-0.2 M magnesium chloride 0.1 M hepes buffer pH 6.5 9-10% PEG4k |
