9SIW

CK1d in complex with IG111

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ELETTRA BEAMLINE 11.2C
Synchrotron site	ELETTRA
Beamline	11.2C
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-05-20
Detector	DECTRIS PILATUS 6M
Wavelength(s)	1
Spacegroup name	P 1 21 1
Unit cell lengths	49.010, 74.080, 89.300
Unit cell angles	90.00, 103.32, 90.00

Refinement procedure

Resolution	47.690 - 1.550
R-factor	0.1582
Rwork	0.157
R-free	0.18360
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	0.945
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX ((1.19.2_4158: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	47.690	1.605
High resolution limit [Å]	1.550	1.550
Rpim	0.031	0.216
Number of reflections	83026	8636
<I/σ(I)>	15.17
Completeness [%]	92.1
Redundancy	2
CC(1/2)	0.999	0.871

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	5	277.15	0.1 M Sodium Malonate, pH 5 15-22% PEG3350