9SCW
Crystal structure of Coxsackie B1 virus-like particle delta-palxa
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2021-07-13 |
| Detector | DECTRIS EIGER2 XE 16M |
| Wavelength(s) | 0.976250 |
| Spacegroup name | P 3 1 2 |
| Unit cell lengths | 343.999, 343.999, 457.065 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 97.040 - 3.200 |
| R-factor | 0.2941 |
| Rwork | 0.293 |
| R-free | 0.30970 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.604 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.21.1_5286) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 97.040 | 3.390 |
| High resolution limit [Å] | 3.200 | 3.200 |
| Number of reflections | 997876 | 160562 |
| <I/σ(I)> | 3 | |
| Completeness [%] | 99.8 | 99.3 |
| Redundancy | 8.6 | 9.3 |
| CC(1/2) | 0.943 | 0.211 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 295 | 0.1M Na-acetate pH 6.5, 1.5M lithium sulfate |
