9S6A
Crystal structure of Arabidopsis thaliana FUT11 complexed to GDP and G0
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALBA BEAMLINE XALOC |
| Synchrotron site | ALBA |
| Beamline | XALOC |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2024-07-13 |
| Detector | DECTRIS PILATUS3 S 6M |
| Wavelength(s) | 0.97926 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 77.663, 41.150, 82.425 |
| Unit cell angles | 90.00, 96.89, 90.00 |
Refinement procedure
| Resolution | 19.960 - 1.410 |
| R-factor | 0.20584 |
| Rwork | 0.205 |
| R-free | 0.22841 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.785 |
| Data reduction software | xia2 |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0431) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 1.490 |
| High resolution limit [Å] | 1.410 | 1.410 |
| Rpim | 0.034 | |
| Number of reflections | 94108 | 12015 |
| <I/σ(I)> | 6.5 | |
| Completeness [%] | 94.3 | 83.1 |
| Redundancy | 2.8 | |
| CC(1/2) | 0.999 | 0.662 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 291 | LiNaK Tris precipitant mix 6 Acetonitrile |
