9S40

SUDV VP40 in complex with LL106

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2022-10-30
Detector	DECTRIS EIGER X 16M
Wavelength(s)	1.000000
Spacegroup name	C 1 2 1
Unit cell lengths	64.405, 91.411, 48.130
Unit cell angles	90.00, 95.64, 90.00

Refinement procedure

Resolution	36.890 - 1.470
R-factor	0.1894
Rwork	0.188
R-free	0.21230
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	0.886
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	47.900	1.470
High resolution limit [Å]	1.440	1.440
Number of reflections	49650	2519
<I/σ(I)>	13.1	1
Completeness [%]	99.8	97.8
Redundancy	6.8	6.6
CC(1/2)	0.990	0.562

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7.2	293	100 mM HEPES 40 mM MgCl2 10% (v/v) PEG400 20% ethylen glycol as cryoprotectant