9RZS

Hen Egg-White Lysozyme (HEWL) complexed with a Lindqvist-type hexavanadate (V6-N3) polyoxometalate

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SOLEIL BEAMLINE PROXIMA 1
Synchrotron site	SOLEIL
Beamline	PROXIMA 1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2025-02-13
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.97857
Spacegroup name	P 43 21 2
Unit cell lengths	76.049, 76.049, 37.049
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	38.020 - 1.680
R-factor	0.1931
Rwork	0.191
R-free	0.22860
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.010
RMSD bond angle	1.278
Data reduction software	XDS (0.7.16)
Data scaling software	Aimless (1.12.16)
Phasing software	PHASER (1.20.1_4487)
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	38.020	1.710
High resolution limit [Å]	1.680	1.680
Number of reflections	333402	623
<I/σ(I)>	21
Completeness [%]	100.0
Redundancy	25.8
CC(1/2)	0.999	0.963

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	4	291	1.0M LiCl, 0.1M Citric acid, 10%(w/v) PEG 6000