9RYD
Room temperature serial structure of CTX-M-15 collected on tape drive at Diamond Light Source VMXi
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE VMXi |
| Synchrotron site | Diamond |
| Beamline | VMXi |
| Temperature [K] | 294 |
| Detector technology | PIXEL |
| Collection date | 2024-01-29 |
| Detector | DECTRIS EIGER2 X 4M |
| Wavelength(s) | 0.7749 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 44.908, 45.553, 117.446 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 58.720 - 1.830 |
| R-factor | 0.1676 |
| Rwork | 0.166 |
| R-free | 0.19940 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.755 |
| Data reduction software | DIALS |
| Data scaling software | DIALS |
| Phasing software | PHENIX |
| Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 58.720 | 1.860 |
| High resolution limit [Å] | 1.830 | 1.830 |
| Number of reflections | 21932 | 1038 |
| <I/σ(I)> | 9.2 | 0.8 |
| Completeness [%] | 99.8 | 98.2 |
| Redundancy | 91.9 | 11.1 |
| CC(1/2) | 0.966 | 0.305 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 8 | 292 | 2.0 M ammonium sulphate, 0.1 M Tris 8.0 |
