Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-2 |
| Synchrotron site | ESRF |
| Beamline | ID23-2 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2020-09-17 |
| Detector | DECTRIS PILATUS3 X 2M |
| Wavelength(s) | 0.87313 |
| Spacegroup name | P 32 |
| Unit cell lengths | 48.445, 48.445, 113.364 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 39.377 - 1.109 |
| Rwork | 0.165 |
| R-free | 0.18540 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.856 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER (7.0.078) |
| Refinement software | REFMAC (5.8.0430) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 39.400 | 1.230 |
| High resolution limit [Å] | 1.100 | 1.110 |
| Number of reflections | 103362 | 2907 |
| <I/σ(I)> | 15 | 0.6 |
| Completeness [%] | 97.4 | 49.7 |
| Redundancy | 9.8 | 7.8 |
| CC(1/2) | 0.999 | 0.143 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 298.5 | 0.2 M ammonium citrate dibasic 20% w/v PEG 3350 (JCSG+ crystallization screen; Molecular Dimensions Ltd., condition A3). |
