9RF6

SUDV VP40 in complex with LL093

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2022-09-02
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.999990
Spacegroup name	C 1 2 1
Unit cell lengths	62.906, 91.136, 47.949
Unit cell angles	90.00, 94.82, 90.00

Refinement procedure

Resolution	47.780 - 1.900
R-factor	0.2288
Rwork	0.228
R-free	0.25100
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	0.978
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	47.780	1.968
High resolution limit [Å]	1.900	1.900
Number of reflections	20853	2085
<I/σ(I)>	5.99	2.43
Completeness [%]	98.0	98.02
Redundancy	6.9	7
CC(1/2)	0.983	0.935

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	100 mM HEPES, 40 mM MgCl2, 10% (v/v) PEG400 cryoprotectant: ethylen glycol