9REV

SUDV VP40 in complex with LL105

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2022-10-30
Detector	DECTRIS EIGER X 16M
Wavelength(s)	1.000000
Spacegroup name	C 1 2 1
Unit cell lengths	64.549, 91.735, 47.827
Unit cell angles	90.00, 95.87, 90.00

Refinement procedure

Resolution	36.860 - 1.540
R-factor	0.1897
Rwork	0.188
R-free	0.21990
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	0.988
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	36.860	1.597
High resolution limit [Å]	1.540	1.540
Number of reflections	40076	3577
<I/σ(I)>	24.94	2.5
Completeness [%]	98.3	87.53
Redundancy	6.6	5.1
CC(1/2)	1.000	0.923

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	100 mM HEPES 40 mM MgCl2 10% (v/v) PEG400 20% ethylen glycol as cryoprotectant