Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2022-10-13 |
| Detector | DECTRIS EIGER2 XE 16M |
| Wavelength(s) | 0.9763 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 68.280, 73.448, 76.901 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 51.060 - 1.130 |
| R-factor | 0.1201 |
| Rwork | 0.119 |
| R-free | 0.14600 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.001 |
| Data reduction software | autoPROC |
| Data scaling software | STARANISO |
| Phasing software | PHENIX |
| Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 53.114 | 1.200 |
| High resolution limit [Å] | 1.130 | 1.130 |
| Rpim | 0.018 | 0.403 |
| Number of reflections | 118632 | 5933 |
| <I/σ(I)> | 18.8 | 1.6 |
| Completeness [%] | 89.5 | |
| Redundancy | 13.4 | |
| CC(1/2) | 1.000 | 0.702 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 292 | 0.1M bis-tris pH 5.8, 32% PEG 3350, 0.15M NH4SO4 |
