9QVB

Structure of Eimeria tenella SAG13 (ETH_00013178)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I03
Synchrotron site	Diamond
Beamline	I03
Temperature [K]	100
Detector technology	PIXEL
Collection date	2023-03-11
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.97623
Spacegroup name	C 2 2 21
Unit cell lengths	49.570, 65.160, 114.600
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	39.483 - 1.750
Rwork	0.188
R-free	0.24510
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.011
RMSD bond angle	1.989
Data reduction software	xia2
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	REFMAC (5.8.0419)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	39.500	1.740
High resolution limit [Å]	1.700	1.700
Rmerge	0.230	2.940
Rpim	0.997	0.300
Number of reflections	20477	982
<I/σ(I)>	7.55	0.82
Completeness [%]	100.0	100
Redundancy	13.25
CC(1/2)	0.997	0.301

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	6.9	290	0.2 M potassium nitrate pH6.9, 20% w/v PEG3350