9QNQ

APH(2'')-Id with a fragment

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID29
Synchrotron site	ESRF
Beamline	ID29
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-11-11
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.9897
Spacegroup name	P 1 21 1
Unit cell lengths	75.787, 65.120, 76.900
Unit cell angles	90.00, 91.68, 90.00

Refinement procedure

Resolution	49.690 - 2.380
R-factor	0.2264
Rwork	0.223
R-free	0.29610
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.009
RMSD bond angle	0.961
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX ((1.20.1_4487: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	49.690	2.460
High resolution limit [Å]	2.380	2.380
Number of reflections	30212	2999
<I/σ(I)>	10.12
Completeness [%]	99.6
Redundancy	4.8
CC(1/2)	0.995	0.808

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		291	12% PEG3350, 50-90 mM Ammonium citrate